Publications by the researcher in collaboration with Christopher Glidewell (254)

2023

  1. Synthesis of 5-(arylmethylideneamino)-4-(1H-benzo[d]imidazol-1-yl)pyrimidine hybrids: synthetic sequence and the molecular and supramolecular structures of two intermediates and three final products

    Acta crystallographica. Section C, Structural chemistry, Vol. 79, pp. 227-236

2021

  1. Synthesis and spectroscopic and structural characterization of spiro[indoline-3,3′-indolizine]s formed by 1,3-dipolar cycloadditions between isatins, pipecolic acid and an electron-deficient alkene

    Acta Crystallographica Section C: Structural Chemistry, Vol. 77, pp. 496-504

2020

  1. 4-Styrylquinolines from cyclocondensation reactions between (2-aminophenyl)chalcones and 1,3-diketones: Crystal structures and regiochemistry

    Acta Crystallographica Section C: Structural Chemistry, Vol. 76, pp. 883-890

  2. Conversion of 3-amino-4-arylamino-1H-isochromen- 1-ones to 1-arylisochromeno[3,4-d]- [1,2,3]triazol-5(1H)-ones: Synthesis, spectroscopic characterization and the structures of four products and one ring-opened derivative

    Acta Crystallographica Section C: Structural Chemistry, Vol. 76, pp. 446-453

  3. Regio- And stereospecific assembly of di­spiro­[indoline-3,3′-pyrrolizine-1′,5′′-thia­zolidines] from simple precursors using a one-pot procedure: Synthesis, spectroscopic and structural characterization, and a proposed mechanism of formation

    Acta Crystallographica Section C: Structural Chemistry, Vol. 76, pp. 779-785

  4. Synthesis of N-substituted 3-(2-aryl-2-oxoethyl)- 3-hydroxyindolin-2-ones and their conversion to N-substituted (E)-3-(2-aryl-2-oxoethylidene)-indolin-2-ones: Synthetic sequence, spectroscopic characterization and structures of four 3-hydroxy compounds and five oxoethylidene products

    Acta Crystallographica Section C: Structural Chemistry, Vol. 76, pp. 433-445

2019

  1. A concise and efficient concurrent synthesis of 6,11-dihydrodibenzo[b,e]azepines and 5,6,11,12-tetrahydrodibenzo[b,f]azocines and their conversion to 4-oxo-8,13-dihydro-4H-benzo[5,6]aze-pino[3,2,1-ij]quinoline-5-carboxylates and N-acetyl-5,6,11,12-tetrahydrodibenzo[b,f]azocines: Synthetic sequence, spectroscopic characterization and the structures of two products

    Acta Crystallographica Section C: Structural Chemistry, Vol. 75, pp. 650-656

  2. A concise and efficient synthesis of amino-substituted (1H-benzo[d]imidazol-1-yl)pyrimidine hybrids: Synthetic sequence and the molecular and supramolecular structures of six examples

    Acta Crystallographica Section C: Structural Chemistry, Vol. 75, pp. 1405-1416

  3. A concise and versatile route to tetrahydro-1-benzazepines carrying [a]-fused heterocyclic units: Synthetic sequence and spectroscopic characterization, and the molecular and supramolecular structures of one intermediate and two products

    Acta Crystallographica Section C: Structural Chemistry, Vol. 75, pp. 168-177

  4. Monoclinic and orthorhombic forms of (Rs)-(e)-4-[2-(4-chlorobenzylidene)hydrazinyl]-6,11-dimethyl-6,11-dihydro-5h-benzo[b]pyrimido[5,4-f]azepine: Synthesis, concomitant polymorphism and supramolecular assembly mediated by C—H…N, C—H…π(arene) and C—CL…π(arene) interactions

    Acta Crystallographica Section C: Structural Chemistry, Vol. 75, pp. 686-693

2018

  1. A concise synthesis of a highly substituted 6-(1H-benzimidazol-1-yl)-5-nitrosopyrimidin-2- amine: Synthetic sequence and the molecular and supramolecular structures of one product and two intermediates

    Acta Crystallographica Section C: Structural Chemistry, Vol. 74, pp. 696-702

2017

  1. Design, synthesis and crystallographic study of novel indole-based cyano derivatives as key building blocks for heteropolycyclic compounds of major complexity

    Acta Crystallographica Section C: Structural Chemistry, Vol. 73, Núm. 12, pp. 1040-1049

  2. Reduced 3,4′-bipyrazoles from a simple pyrazole precursor: Synthetic sequence, molecular structures and supramolecular assembly

    Acta Crystallographica Section C: Structural Chemistry, Vol. 73, Núm. 10, pp. 784-790

  3. Synthesis of spiro[indoline-3,3′-pyrrolizines] by 1,3-dipolar reactions between isatins, l -proline and electron-deficient alkenes

    Acta Crystallographica Section C: Structural Chemistry, Vol. 73, Núm. 12, pp. 1109-1115

  4. Three tetracyclic dibenzoazepine derivatives exhibiting different molecular conformations, different patterns of intermolecular hydrogen bonding and different modes of supramolecular aggregation

    Acta Crystallographica Section C: Structural Chemistry, Vol. 73, Núm. 1, pp. 28-35

2016

  1. Diastereoisomeric forms of 11-ethyl-6,11-dihydro-5H-dibenzo[b,e]azepine-6-carboxamide: syntheses and the molecular and supramolecular structure of the minor form (6RS,11RS)-11-ethyl-6,11-dihydro-5H-dibenzo[b,e]azepine-6-carboxamide

    Acta Crystallographica Section C: Structural Chemistry, Vol. 72, Núm. 7, pp. 549-554

  2. Similar molecular constitutions but different conformations and different supramolecular assemblies in two related fused tetracyclic benzo[b]pyrimido[5,4-f]azepine derivatives

    Acta Crystallographica Section C: Structural Chemistry, Vol. 72, pp. 52-56

  3. Six polycyclic pyrimidoazepine derivatives: Syntheses, molecular structures and supramolecular assembly

    Acta Crystallographica Section C: Structural Chemistry, Vol. 72, Núm. 4, pp. 346-357

  4. Unexpected ring-closure products derived from 3-(2-allylanilino)-3-phenylacrylate esters: Crystal and molecular structures of 3-acetyl-8-allyl-6-methyl-2-phenylquinolin-4-yl acetate and (2RS)-2,8-dimethyl-4-phenyl-1,2-dihydro-6H-pyrrolo[3,2,1-ij]quinolin-6-one

    Acta Crystallographica Section C: Structural Chemistry, Vol. 72, Núm. 8, pp. 619-626

2015

  1. (5RS)-6H-Spiro[pyrazolo[1,5-c]quinazoline-5,4′-thiochroman]: Efficient synthesis under mild conditions, molecular structure and supramolecular assembly

    Acta Crystallographica Section C: Structural Chemistry, Vol. 71, pp. 1028-1032