GRUPO INVESTIGACION EN COMPUESTOS INTERES BIOLOGICO (GICIB)
University of St Andrews
Saint Andrews, Reino UnidoPublicaciones en colaboración con investigadores/as de University of St Andrews (238)
2023
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Synthesis of 5-(arylmethylideneamino)-4-(1H-benzo[d]imidazol-1-yl)pyrimidine hybrids: synthetic sequence and the molecular and supramolecular structures of two intermediates and three final products
Acta crystallographica. Section C, Structural chemistry, Vol. 79, pp. 227-236
2022
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Synthesis and spectroscopic and structural characterization of three new 2-methyl-4-styrylquinolines formed using Friedländer reactions between (2-aminophenyl)chalcones and acetone
Acta crystallographica. Section C, Structural chemistry, Vol. 78, pp. 524-530
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Synthesis, and spectroscopic and structural characterization of three new styrylquinoline-benzimidazole hybrids
Acta crystallographica. Section C, Structural chemistry, Vol. 78, pp. 671-680
2021
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Synthesis and spectroscopic and structural characterization of spiro[indoline-3,3′-indolizine]s formed by 1,3-dipolar cycloadditions between isatins, pipecolic acid and an electron-deficient alkene
Acta Crystallographica Section C: Structural Chemistry, Vol. 77, pp. 496-504
2020
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4-Styrylquinolines from cyclocondensation reactions between (2-aminophenyl)chalcones and 1,3-diketones: Crystal structures and regiochemistry
Acta Crystallographica Section C: Structural Chemistry, Vol. 76, pp. 883-890
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Conversion of 3-amino-4-arylamino-1H-isochromen- 1-ones to 1-arylisochromeno[3,4-d]- [1,2,3]triazol-5(1H)-ones: Synthesis, spectroscopic characterization and the structures of four products and one ring-opened derivative
Acta Crystallographica Section C: Structural Chemistry, Vol. 76, pp. 446-453
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Regio- And stereospecific assembly of dispiro[indoline-3,3′-pyrrolizine-1′,5′′-thiazolidines] from simple precursors using a one-pot procedure: Synthesis, spectroscopic and structural characterization, and a proposed mechanism of formation
Acta Crystallographica Section C: Structural Chemistry, Vol. 76, pp. 779-785
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Synthesis of N-substituted 3-(2-aryl-2-oxoethyl)- 3-hydroxyindolin-2-ones and their conversion to N-substituted (E)-3-(2-aryl-2-oxoethylidene)-indolin-2-ones: Synthetic sequence, spectroscopic characterization and structures of four 3-hydroxy compounds and five oxoethylidene products
Acta Crystallographica Section C: Structural Chemistry, Vol. 76, pp. 433-445
2019
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A concise and efficient concurrent synthesis of 6,11-dihydrodibenzo[b,e]azepines and 5,6,11,12-tetrahydrodibenzo[b,f]azocines and their conversion to 4-oxo-8,13-dihydro-4H-benzo[5,6]aze-pino[3,2,1-ij]quinoline-5-carboxylates and N-acetyl-5,6,11,12-tetrahydrodibenzo[b,f]azocines: Synthetic sequence, spectroscopic characterization and the structures of two products
Acta Crystallographica Section C: Structural Chemistry, Vol. 75, pp. 650-656
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A concise and efficient synthesis of amino-substituted (1H-benzo[d]imidazol-1-yl)pyrimidine hybrids: Synthetic sequence and the molecular and supramolecular structures of six examples
Acta Crystallographica Section C: Structural Chemistry, Vol. 75, pp. 1405-1416
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A concise and versatile route to tetrahydro-1-benzazepines carrying [a]-fused heterocyclic units: Synthetic sequence and spectroscopic characterization, and the molecular and supramolecular structures of one intermediate and two products
Acta Crystallographica Section C: Structural Chemistry, Vol. 75, pp. 168-177
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Monoclinic and orthorhombic forms of (Rs)-(e)-4-[2-(4-chlorobenzylidene)hydrazinyl]-6,11-dimethyl-6,11-dihydro-5h-benzo[b]pyrimido[5,4-f]azepine: Synthesis, concomitant polymorphism and supramolecular assembly mediated by C—H…N, C—H…π(arene) and C—CL…π(arene) interactions
Acta Crystallographica Section C: Structural Chemistry, Vol. 75, pp. 686-693
2018
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A concise synthesis of a highly substituted 6-(1H-benzimidazol-1-yl)-5-nitrosopyrimidin-2- amine: Synthetic sequence and the molecular and supramolecular structures of one product and two intermediates
Acta Crystallographica Section C: Structural Chemistry, Vol. 74, pp. 696-702
2017
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Design, synthesis and crystallographic study of novel indole-based cyano derivatives as key building blocks for heteropolycyclic compounds of major complexity
Acta Crystallographica Section C: Structural Chemistry, Vol. 73, Núm. 12, pp. 1040-1049
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Reduced 3,4′-bipyrazoles from a simple pyrazole precursor: Synthetic sequence, molecular structures and supramolecular assembly
Acta Crystallographica Section C: Structural Chemistry, Vol. 73, Núm. 10, pp. 784-790
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Synthesis of spiro[indoline-3,3′-pyrrolizines] by 1,3-dipolar reactions between isatins, l -proline and electron-deficient alkenes
Acta Crystallographica Section C: Structural Chemistry, Vol. 73, Núm. 12, pp. 1109-1115
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Three tetracyclic dibenzoazepine derivatives exhibiting different molecular conformations, different patterns of intermolecular hydrogen bonding and different modes of supramolecular aggregation
Acta Crystallographica Section C: Structural Chemistry, Vol. 73, Núm. 1, pp. 28-35
2016
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Diastereoisomeric forms of 11-ethyl-6,11-dihydro-5H-dibenzo[b,e]azepine-6-carboxamide: syntheses and the molecular and supramolecular structure of the minor form (6RS,11RS)-11-ethyl-6,11-dihydro-5H-dibenzo[b,e]azepine-6-carboxamide
Acta Crystallographica Section C: Structural Chemistry, Vol. 72, Núm. 7, pp. 549-554
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Similar molecular constitutions but different conformations and different supramolecular assemblies in two related fused tetracyclic benzo[b]pyrimido[5,4-f]azepine derivatives
Acta Crystallographica Section C: Structural Chemistry, Vol. 72, pp. 52-56
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Six polycyclic pyrimidoazepine derivatives: Syntheses, molecular structures and supramolecular assembly
Acta Crystallographica Section C: Structural Chemistry, Vol. 72, Núm. 4, pp. 346-357